
80 mm Diameter Molecular Distillation Equipment for CBD / THC / Hemp oi l/ Cannabissativa
—— Operation
Feed liquid is admitted into still under high vacuum, immediately spread into a very thin film and forced quickly down the evaporation surface. Heated walls and high vacuum drive the more volatile components (distillate) to the external condenser as the less volatile components (residue) continue down the cylinder. The resulting fractions, thus separated, exit through individual discharge outlets. Depending on application, the desired product is either the distillate or the residue fraction. Small amounts of condensable low MW compounds collect in cold trap upstream of vacuum system. For high solvent loads, an optional external condenser may be installed immediately downstream of the still.
The process of distillation when carried out in an apparatus designed for high vacuum in order to allow the molecules escape from the warm liquid into a cooler surface inside a condenser before coming in contact with other molecules and finally settle down into the liquid is known as molecular distillation. The molecular distillation is applied to purify low volatile substances.
The molecular distillation was developed before the Second World War to distill heat sensitive natural products like vitamins. These process were carried out in United States under Dr Hickman, the inventor of the method. He derived this method with a simple lab equipment. A thin layer of product was heated in a tray under high vacuum and the vapour was condensed on the surrounding cold surface.
The operating conditions were set in a manner that the free path of the molecules was longer than the distance between heated and cooled surface. The probability of a vapour molecule colliding with another molecule was less than the probability to travel without collision to cold surface.
TYPE | DZL-5 |
MATERIAL | stainless steel 316 |
TEMPERATURE | Room temp~200/300 ℃(depend on the Electric heater) |
DIAMETER | 80 (mm) |
HEAT EXCHANGER HTA | 0.058 (m2) |
INNER CONDENSING HTA | 0.065 (m2) |
FEED AMOUNT | 2000~6000 ( ml/h) |
ROTATION SPEED | 80-390rpm |
FILM SYSTEM | Wiped Filming System |
VACUITY | 0.001mbar(depend on the nature of material and vacuum pump) |
COLD TRAP | Liquid nitrogen |
FLOOR AREA | length*width*height=1100*500*1750 (mm)(without pump) |
POWER | 2KW (without pump) |
VOLTAGE | 220V-60HZ |
Shanghai Dea Chemical Equipment Co., Ltd.
Shanghai Dea chemical equipment Co.,Ltd
—— We devote to design and develop the equipment of chemical separation and abstraction.
—— We came from East China University of Science and Technology, which we long-term cooperated with later. And now, we serve for many famous universities, such as Tsinghua University , Sun Yat-sen University , etc.
—— We provide equipment of distillation and extraction for the technicians in the area of chemical medicine and food industry.
—— We own senior engineers who have rich experience in chemical engineering.
—— Our products can be used in lab-scale, pilot-scale experiments and small-scale production.
—— The experimental results are more authentic by using our products thanks to the continuous operation during the course of the experiments or pilot-scale experiments.
—— We repaire imputed equipments out-of-warranty for UIC,POPE,BUCHI in the past few years, which made us accumulating rich experience.
—— Practical, quality first, service first, reputation first' is the motto that guides the work of DEA team.