
Plant Oil Molecular Distillation Equipment With PLC Automatic
Control System
Molecular Distillation Equipment Application
1. Thermal separation of heat sensitive chemical compounds.
2. The purification of organic synthetic material.
3. The separation of effective components from the biological
extracting solution.
4. The recycling of industrial waste.
5. Remove toxic substances in the food industry.
6. The organic compounds' decoloring, and eliminate the unusual
smell.
7. High precision to remove residual solvent in chemical compound.
Molecular Distillation Equipment Operation
Feed liquid is admitted into still under high vacuum, immediately
spread into a very thin film and forced quickly down the
evaporation surface. Heated walls and high vacuum drive the more
volatile components (distillate) to the external condenser as the
less volatile components (residue) continue down the cylinder. The
resulting fractions, thus separated, exit through individual
discharge outlets. Depending on application, the desired product is
either the distillate or the residue fraction. Small amounts of
condensable low MW compounds collect in cold trap upstream of
vacuum system. For high solvent loads, an optional external
condenser may be installed immediately downstream of the still.
Molecular distillation is a type of short-path vacuum distillation,
characterized by an extremely low vacuum pressure, 0.01 torr or
below.It is a process of separation, purification and concentration
of natural products, complex and thermally sensitive molecules for
example vitamins and polyunsaturated fatty acids. This process is
characterized by short term exposure of the distillate liquid to
high temperatures in high vacuum (around 10−4 mmHg) in the
distillation column and a small distance between the evaporator and
the condenser around 2 cm.In molecular distillation, fluids are in
the free molecular flow regime, i.e. the mean free path of
molecules is comparable to the size of the equipment.The gaseous
phase no longer exerts significant pressure on the substance to be
evaporated, and consequently, rate of evaporation no longer depends
on pressure. The motion of molecules is in the line of sight,
because they do not form a continuous gas anymore. Thus, a short
path between the hot surface and the cold surface is necessary,
typically by suspending a hot plate covered with a film of feed
next to a cold plate with a line of sight in between.
This process has the advantages of avoiding the problem of toxicity
that occurs in techniques that use solvents as the separating
agent, and also of minimizing losses due to thermal decomposition.
and can be used in a continuous feed process to harvest distillate
without having to break vacuum.
TYPE | DZL-5 Molecular Distillation Equipment |
MATERIAL | stainless steel 316 |
TEMPERATURE | Room temp~200/300 ℃(depend on the Electric heater) |
DIAMETER | 80 (mm) |
HEAT EXCHANGER HTA | 0.058 (m2) |
INNER CONDENSING HTA | 0.065 (m2) |
FEED AMOUNT | 2000~6000 ( ml/h) |
ROTATION SPEED | 80-390rpm |
FILM SYSTEM | Wiped Filming System |
VACUITY | 0.001mbar(depend on the nature of material and vacuum pump) |
COLD TRAP | Liquid nitrogen |
FLOOR AREA | length*width*height=1100*500*1750 (mm)(without pump) |
POWER | 2KW (without pump) |
VOLTAGE | 220V-60HZ |
Shanghai Dea Chemical Equipment Co., Ltd.
Shanghai Dea chemical equipment Co.,Ltd
—— We devote to design and develop the equipment of chemical separation and abstraction.
—— We came from East China University of Science and Technology, which we long-term cooperated with later. And now, we serve for many famous universities, such as Tsinghua University , Sun Yat-sen University , etc.
—— We provide equipment of distillation and extraction for the technicians in the area of chemical medicine and food industry.
—— We own senior engineers who have rich experience in chemical engineering.
—— Our products can be used in lab-scale, pilot-scale experiments and small-scale production.
—— The experimental results are more authentic by using our products thanks to the continuous operation during the course of the experiments or pilot-scale experiments.
—— We repaire imputed equipments out-of-warranty for UIC,POPE,BUCHI in the past few years, which made us accumulating rich experience.
—— Practical, quality first, service first, reputation first' is the motto that guides the work of DEA team.